Polymethylaluminoxane supported zirconocene catalysts for polymerisation of ethylene

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IN SITU SILICA SUPPORTED METALLOCENE CATALYSTS FOR ETHYLENE POLYMERIZATION

Bis(2-R-ind)ZrCl2 (R: H or phenyl) was supported on different types of silica by in situ impregnation method and used for ethylene polymerization. In this method, the step of catalyst loading on support was eliminated and common alkyl aluminum (triisobutylaluminum, TiBA) cocatalyst was used instead of expensive methyl aluminiumoxane (MAO) cocatalyst in the polymerization. The effect of surface ...

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Mesoporous silica-supported zirconocene catalysts for highly isotactic polypropylene.

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in situ silica supported metallocene catalysts for ethylene polymerization

bis(2-r-ind)zrcl2 (r: h or phenyl) was supported on different types of silica by in situ impregnation method and used for ethylene polymerization. in this method, the step of catalyst loading on support was eliminated and common alkyl aluminum (triisobutylaluminum, tiba) cocatalyst was used instead of expensive methyl aluminiumoxane (mao) cocatalyst in the polymerization. the effect of surface ...

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Borane-functionalized silica supports In situ activated heterogeneous zirconocene catalysts for MAO-free ethylene polymerization

We treated silica with tris(pentafluorophenyl)borane, B(C6F5)3, to create borane-functionalized support, SiO2–B(C6F5)3 which was then used as a support and co-catalyst for the in situ activated dichloro-zirconocene (Cp2ZrCl2/TIBA) and dimethyl-zirconocene catalyst systems (Cp2Zr(CH3)2) for ethylene polymerization. The surface modifications of SiO2– B(C6F5)3 was investigated by SEM–EDX, FTIR and...

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Imido-modified SiO2-supported Ti/Mg Ziegler-Natta catalysts for ethylene polymerization and ethylene/1-hexene copolymerization

A novel imido-modified SiO2-supported Ti/Mg Ziegler-Natta catalyst for ethylene and ethylene/1-hexene polymerization is investigated. The catalyst is prepared by modification of (SiO2/MgO/MgCl2)TiClx Ziegler-Natta catalysts via supporting vanadium species followed by reaction with p-tolyl isocyanate as imido agents, to get the merits from both the SiO2-supported imido vanadium catalyst and the ...

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ژورنال

عنوان ژورنال: Journal of Organometallic Chemistry

سال: 2016

ISSN: 0022-328X

DOI: 10.1016/j.jorganchem.2016.08.015